4-甲烷磺酰基-3-硝基-苯甲酸合成路线 （共 5 条）
反应条件
OxoneR in methanol; water
T=5 - 20°C; 0.0833333 h;
参考文献
SCHERING AKTIENGESELLSCHAFT
Patent: WO2004/48343 A1, 2004 ;
Location in patent: Page 109 ;
WO 2004/048343 A1
反应条件
dihydrogen peroxide in water; acetic acid
参考文献
BASF Aktiengesellschaft
Patent: US6262074 B1, 2001 ;
反应条件
lithium hydroxide hydrate in tetrahydrofuran
T=20°C;
参考文献
Hwang, Jong Yeon; Attia, Ramy R.; Carrillo, Angela K.; Connelly, Michele C.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1891 - 1895
反应条件
1: tetrahydrofuran / 50 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
3: lithium hydroxide hydrate / tetrahydrofuran / 20 °C
View Scheme
参考文献
Hwang, Jong Yeon; Attia, Ramy R.; Carrillo, Angela K.; Connelly, Michele C.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1891 - 1895
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
2: lithium hydroxide hydrate / tetrahydrofuran / 20 °C
View Scheme
参考文献
Hwang, Jong Yeon; Attia, Ramy R.; Carrillo, Angela K.; Connelly, Michele C.; Guy, R. Kiplin
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1891 - 1895
