反应条件
1: 80 percent / 0.58 h / 180 °C / sealed tube
2: 90 percent / LiAlH4 / diethyl ether / a. reflux while adding reagent b. overnight room temperature c. 1h reflux
3: Et3N / CH2Cl2 / 0 °C
4: 1.) cuprous iodide / 1.) Et2O, -10 deg C, 1o min 2. 4h, 0 deg C
5: 80 percent / PTS / methanol / 4 h
View Scheme
参考文献
Vig, O. P.; Sharma, M. L.; Verma, N. K.; Malik, Neera
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 10 p. 860 - 862
