in ethanol the disulfide was added to suspn. of Hg-complex in EtOH in a Schlenk tube; soln. was stirred for 12 h in the dark at 50°C; evapd. to dryness; residue was washed with cold EtOH and dried in vacuo;

暂无反应条件数据

T=-14 - 0°C;

T=190°C;

tetrabutylammomium bromide in chloroform Ar-atmosphere; stirring (room temp., 2 min), PhCOCl addn., stirring (5 h); evapn. (vac.), EtOAc addn., filtering, evapn., chromy. (SiO2, hexanes, EtOAc);