1,1,1-三氟-2-十五烷酮合成路线 (共 4 条)
反应条件
pyridine in toluene
T=0 - 20°C;
参考文献
Li, Qingjiang; Tochtrop, Gregory P.
Organic Letters, 2014 , vol. 16, # 5 p. 1382 - 1385
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; pentane
24 h; Ambient temperature;
参考文献
Wiedemann, Juergen; Heiner, Thomas; Mloston, Gregorz; Prakash, G.K. Surya; Olah, George A.
Angewandte Chemie - International Edition, 1998 , vol. 37, # 6 p. 820 - 821
反应条件
1: (COCl)2 / CH2Cl2 / 3 h / 25 °C
2: pyridine / diethyl ether
View Scheme
参考文献
Boger, Dale L.; Sato, Haruhiko; Lerner, Aaron E.; Austin, Bryce J.; Patterson, Jean E.; Patricelli, Matthew P.; Cravatt, Benjamin F.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 2 p. 265 - 270
反应条件
pyridine in diethyl ether
参考文献
Boger, Dale L.; Sato, Haruhiko; Lerner, Aaron E.; Austin, Bryce J.; Patterson, Jean E.; Patricelli, Matthew P.; Cravatt, Benjamin F.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 2 p. 265 - 270