3,4-二甲基-5-戊基-2-呋喃壬酸甲酯合成路线 （共 8 条）
反应条件
1: 25.7 percent / SnCl4 / CHCl3 / 6 h / -50 °C
2: hydrazinhydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
3: diethyl ether
View Scheme
参考文献
Schoedel, Rolf; Spiteller, Gerhard
Helvetica Chimica Acta, 1985 , vol. 68, p. 1624 - 1634
反应条件
1: 25.7 percent / SnCl4 / CHCl3 / 6 h / -50 °C
2: hydrazinhydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
3: diethyl ether
View Scheme
参考文献
Schoedel, Rolf; Spiteller, Gerhard
Helvetica Chimica Acta, 1985 , vol. 68, p. 1624 - 1634
反应条件
1: hydrazinhydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
2: diethyl ether
View Scheme
参考文献
Schoedel, Rolf; Spiteller, Gerhard
Helvetica Chimica Acta, 1985 , vol. 68, p. 1624 - 1634
反应条件
boron trifluoride in methanol
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
反应条件
1: H2SO4 / methanol
2: KOH / dimethylsulfoxide
3: BF3 / methanol
View Scheme
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
反应条件
1: KOH / dimethylsulfoxide
2: BF3 / methanol
View Scheme
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
反应条件
in diethyl ether
Yield given;
参考文献
Schoedel, Rolf; Spiteller, Gerhard
Helvetica Chimica Acta, 1985 , vol. 68, p. 1624 - 1634
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jie, Marcel S. F. Lie Ken; Ahmad, Fasih
Journal of the Chemical Society, Chemical Communications, 1981 , # 21 p. 1110 - 1111
