(1-乙氧基乙烯基)-三甲基硅烷合成路线 (共 4 条)
反应条件
tert.-butyl lithium 1.) THF, pentan, from -78 to -25 deg C, 2.) -78 deg C, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 50, # 25 p. 5410 - 5413
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 41, p. 609 - 613,606 - 609
反应条件
tert.-butyl lithium 1.) pentane, THF, -25 deg C, 2 h, 2.) -78 deg C -> 20 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 1763 - 1768
反应条件
hydrogenchloride in diethyl ether 1.5 h; Yield given;
参考文献
Cunico, Robert F.; Kuan, Chia-Piao
Journal of Organic Chemistry, 1985 , vol. 50, # 25 p. 5410 - 5413