3-(全氟正丁烷)-1,2-环氧丙烷合成路线 (共 8 条)
反应条件
potassium hydroxide in hexane 2.5 h; Heating; Yields of byproduct given;
参考文献
Cirkva, Vladimir; Ameduri, Bruno; Boutevin, Bernard; Paleta, Oldrich
Journal of Fluorine Chemistry, 1997 , vol. 83, # 2 p. 151 - 158
反应条件
potassium hydroxide; 2,2'-azo-bisisobutyronitrile in 1,2-dichloro-ethane T=70°C; Substitution; Cyclization; Dimerization; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 106, # 1 p. 1 - 5
反应条件
potassium hydroxide in hexane 16 h; Heating;
参考文献
Guyot, Bernard; Ameduri, Bruno; Boutevin, Bernard
Journal of Fluorine Chemistry, 1995 , vol. 74, # 2 p. 233 - 240
反应条件
potassium hydroxide in dichloromethane 1 h; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 64, # 1-2 p. 125 - 128
反应条件
potassium hydroxide in diethyl ether 5 h; Heating; Yields of byproduct given;
参考文献
Cirkva, Vladimir; Ameduri, Bruno; Boutevin, Bernard; Paleta, Oldrich
Journal of Fluorine Chemistry, 1997 , vol. 83, # 2 p. 151 - 158
反应条件
potassium hydroxide; 2,6-di-t-butyl-4-methyl-phenol 2.) hexane, reflux, 3 h; Yield given. Multistep reaction;
参考文献
Journal of Fluorine Chemistry, , vol. 83, # 2 p. 151 - 158
反应条件
potassium hydroxide; 2,6-di-t-butyl-4-methyl-phenol 2.) Et2O, reflux, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 83, # 2 p. 151 - 158
反应条件
1: 95 percent / BF3*Et2O / 0.5 h / Heating 2: 96 percent / aq. HCl, MeOH / 2 h / Heating View Scheme
参考文献
Cirkva, Vladimir; Ameduri, Bruno; Boutevin, Bernard; Paleta, Oldrich
Journal of Fluorine Chemistry, 1997 , vol. 84, # 1 p. 53 - 61