2,2,2-三氟-1,1-二甲基-乙胺合成路线 (共 2 条)
反应条件
1: methyllithium With cerium(III) chloride in diethyl ether
T=-78°C; 0.5 h;
2: trifluoromethyl amino ketone in tetrahydrofuran; diethyl ether
T=-78 - 20°C;
参考文献
Zhang, Nan; Ayral-Kaloustian, Semiramis
Journal of Fluorine Chemistry, 2002 , vol. 117, # 1 p. 9 - 11
反应条件
sulfur(IV) fluoride; hydrogen fluoride
参考文献
Raasch,M.S.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1406 - 1409