1: dimethyl(phenyl)silyl chloride With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: With iso-propylmagnesium bromide in tetrahydrofuran; 2-methyl tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 3: ClMe2Si–SiMe2–SiMe2Cl in tetrahydrofuran; 2-methyl tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Klausen, Rebekka S.; Widawsky, Jonathan R.; Steigerwald, Michael L.; Venkataraman, Latha; Nuckolls, Colin
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4541 - 4544
1: dimethyl(phenyl)silyl chloride With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: With iso-propylmagnesium bromide in tetrahydrofuran; 2-methyl tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 3: ClMe2Si–SiMe2–SiMe2Cl in tetrahydrofuran; 2-methyl tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Klausen, Rebekka S.; Widawsky, Jonathan R.; Steigerwald, Michael L.; Venkataraman, Latha; Nuckolls, Colin
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4541 - 4544
hydrogenchloride; AlCl3, aluminium chloride in benzene
T=20°C; 2 h;
参考文献
Klausen, Rebekka S.; Widawsky, Jonathan R.; Steigerwald, Michael L.; Venkataraman, Latha; Nuckolls, Colin
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4541 - 4544
