2H-,2H-,3H-,3H-全氟癸酸合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=18°C; 16 h;
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: (i) AcOEt, (ii) HCl, Zn, EtOH
2: aq. KOH / ethanol
View Scheme
参考文献
Brace,N.O.
Journal of Organic Chemistry, 1962 , vol. 27, p. 4491 - 4498
反应条件
hydrogen; palladium on activated charcoal in ethanol
15 h;
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: dimethylformamide / 15 h / 110 °C
2: aq. H2SO4 / 15 h / 120 °C
3: H2 / Pd-C / ethanol / 15 h
View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: aq. H2SO4 / 15 h / 120 °C
2: H2 / Pd-C / ethanol / 15 h
View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
potassium hydroxide in ethanol
参考文献
Brace,N.O.
Journal of Organic Chemistry, 1962 , vol. 27, p. 4491 - 4498
