反应条件
1: 83 percent / diethyl ether / 2 h / -10 °C
2: 84 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 8 h / Ambient temperature
3: 85 percent / 10percent HCl / tetrahydrofuran / 44 h / Heating
4: 74 percent / anhyd. K2CO3 / ethanol / 2.5 h / Heating
5: 37 percent / LiAlH4 / diethyl ether / 1.) r.t., 5 h, 2.) reflux, 4 h
View Scheme
参考文献
Imanishi; Yagi; Hanaoka
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 4 p. 1243 - 1253