7-氨基-1,3-二甲基-3,7-二氢-1H-嘌呤-2,6-二酮合成路线 （共 7 条）
反应条件
hydrogenchloride; sodium nitrite in water T=5°C; 1 h;
参考文献
Kuz'menko, V. V.; Gulevskaya, A. V.; Pozharskii, A. F.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1373 - 1377
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1524 - 1529
反应条件
potassium permanganate; sulfuric acid T=80°C; 2 h; other oxidizing agents;
参考文献
Gulevskaya, A. V.; Kuz'menko, V. V.; Pozharskii, A. F.; Kuz'menko, T.A.; Shorshnev, S. V.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 1 p. 81 - 88
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 1 p. 95 - 102
反应条件
potassium hydroxide; sodium hydroxylamine-O-sulfonate in water
T=60°C; 1 h;
参考文献
Shorshnev, S. V.; Esipov, S. E.; Chernyshev, A. I.; Pozharskii, A. F.; Nanavyan, I. M.; Kuz'menko, V. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 11 p. 1247 - 1251
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 11 p. 1555 - 1559
参考文献
Kloetzer, Wilhelm; Baldinger, Helga; Karpitschka, Eva Maria; Knoflach, Johann
Synthesis, 1982 , # 7 p. 592 - 595
反应条件
in N,N-dimethyl-formamide
T=20°C; 3 h;
参考文献
Kuz'menko, V. V.; Gulevskaya, A. V.; Pozharskii, A. F.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1373 - 1377
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1524 - 1529
反应条件
1: 67 percent / KOH, NH2OSO3H, NaHCO3 / H2O / 0.17 h / 50 °C
2: 99 percent / KOH / ethanol / 0.08 h / Heating
3: 46 percent / dimethylformamide / 3 h / 20 °C
View Scheme
参考文献
Kuz'menko, V. V.; Gulevskaya, A. V.; Pozharskii, A. F.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1373 - 1377
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1524 - 1529
反应条件
1: 99 percent / KOH / ethanol / 0.08 h / Heating
2: 46 percent / dimethylformamide / 3 h / 20 °C
View Scheme
参考文献
Kuz'menko, V. V.; Gulevskaya, A. V.; Pozharskii, A. F.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1373 - 1377
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1524 - 1529
