4-(3,5-二甲基吡唑)-苯甲酸合成路线 (共 4 条)
反应条件
in isopropyl alcohol 15 h; Heating / reflux;
参考文献
METHYLGENE, INC.
Patent: WO2005/30704 A1, 2005 ;
Location in patent: Page/Page column 230 ;
反应条件
in ethanol; acetylacetone
参考文献
MethylGene, Inc.
Patent: US6897220 B2, 2005 ;
US 6897220 B2
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane
T=20°C; 18 h;
参考文献
American Cyanamid Company
Patent: US6831079 B1, 2004 ;
Location in patent: Page/Page column 53 ;
US 6831079 B1
反应条件
in N-methyl-acetamide; hexane; dichloromethane
参考文献
Wyeth
Patent: US6511974 B1, 2003 ;
US 6511974 B1