(三氟甲基)三甲基硅烷合成路线 （共 455 条）
反应条件
1: m-carboxybenzenediazonium tetrafluoroborate With copper(I) isothiocyanate; sodium isothiocyanate; caesium carbonate in acetonitrile T=20°C; 0.166667 h; Inert atmosphere; 2: (trifluoromethyl)-trimethylsilane in acetonitrile T=20°C; 16 h;
参考文献
Danoun, Gregory; Bayarmagnai, Bilguun; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemical Science, 2014 , vol. 5, # 4 p. 1312 - 1316
反应条件
potassium fluoride; silver trifluoromethanesulfonate in 1,2-dichloro-ethane T=85°C; 24 h; Inert atmosphereDarkness;
参考文献
Ye, Yingda; Lee, Shin Hee; Sanford, Melanie S.
Organic Letters, 2011 , vol. 13, # 20 p. 5464 - 5467
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; cyclohexyl BrettPhos; sodium lauryl sulfate; cesium fluoride in toluene T=110°C; 12 h; Inert atmosphere;
参考文献
Samant, Bhupesh S.; Kabalka, George W.
Chemical Communications, 2011 , vol. 47, # 25 p. 7236 - 7238
反应条件
C6H5O(1-)*C13H27KO6(1+) in tetrahydrofuran T=0°C; 1 h; Inert atmosphere;
参考文献
Hatano, Manabu; Suzuki, Shinji; Takagi, Eri; Ishihara, Kazuaki
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3171 - 3174
反应条件
[Bu4N]+[(MeO)2P(O)O]- in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Prakash, G.K. Surya; Panja, Chiradeep; Vaghoo, Habiba; Surampudi, Vijayalakshmi; Kultyshev, Roman; Mandal, Mihirbaran; Rasul, Golam; Mathew, Thomas; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6806 - 6813
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0.5 h;
参考文献
Odinokov; Savchenko; Nazmeeva; Galyautdinov; Khalilov
Russian Chemical Bulletin, 2002 , vol. 51, # 10 p. 1937 - 1939
反应条件
potassium fluoride; tetrabutylammomium bromide in N,N-dimethyl-formamide T=0 - 20°C; Inert atmosphere;
参考文献
Shidlovskii, Alexander F.; Golubev, Alexander S.; Gusev, Dmitrii V.; Suponitsky, Kyrill Yu.; Peregudov, Alexander S.; Chkanikov, Nikolai D.
Journal of Fluorine Chemistry, 2012 , vol. 143, p. 272 - 280,9
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Yoshimatsu, Mitsuhiro; Kuribayashi, Masako
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 11 p. 1256 - 1257
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
参考文献
Yoshimatsu, Mitsuhiro; Kuribayashi, Masako
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 11 p. 1256 - 1257
反应条件
[Bu4N]+[(MeO)2P(O)O]- in N,N-dimethyl-formamide T=20°C; 0.5 h;
参考文献
Prakash, G.K. Surya; Panja, Chiradeep; Vaghoo, Habiba; Surampudi, Vijayalakshmi; Kultyshev, Roman; Mandal, Mihirbaran; Rasul, Golam; Mathew, Thomas; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 6806 - 6813
