(三氟甲基)三甲基硅烷合成路线 （共 455 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0 deg C, 5 min then rt., 2.5 h;
参考文献
Billard, Thierry; Large, Sylvie; Langlois, Bernard R.
Tetrahedron Letters, 1997 , vol. 38, # 1 p. 65 - 68
反应条件
sodium iodide in tetrahydrofuran T=65°C; 2 h; Inert atmosphere;
参考文献
Wang, Fei; Luo, Tao; Hu, Jinbo; Wang, Ying; Krishnan, Hema S.; Jog, Parag V.; Ganesh, Somesh K.; Prakash, G. K. Surya; Olah, George A.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 31 p. 7153 - 7157
反应条件
tetramethyl-ammonium fluoride in ethylene glycol dimethyl ether T=-30 - 20°C;
参考文献
Babadzhanova; Kirij; Yagupolskii; Tyrra; Naumann
Tetrahedron, 2005 , vol. 61, # 7 p. 1813 - 1819
反应条件
tetramethyl-ammonium fluoride in ethylene glycol dimethyl ether T=-30 - 20°C;
参考文献
Babadzhanova; Kirij; Yagupolskii; Tyrra; Naumann
Tetrahedron, 2005 , vol. 61, # 7 p. 1813 - 1819
反应条件
tetramethyl-ammonium fluoride in ethylene glycol dimethyl ether T=-30 - 20°C;
参考文献
Babadzhanova; Kirij; Yagupolskii; Tyrra; Naumann
Tetrahedron, 2005 , vol. 61, # 7 p. 1813 - 1819
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Krishnamurti, Ramesh; Bellew, Donald R.; Prakash, G. K. Surya
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 984 - 989
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=20°C; 4 h; 2: With water in N,N-dimethyl-formamide 4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=20°C; 4 h; 2: With tetrabutyl ammonium fluoride in N,N-dimethyl-formamide 4 h;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
potassium fluoride in N,N-dimethyl acetamide T=50°C; Title compound not separated from byproducts;
参考文献
Adams, Dave J.; Clark, James H.; Hansen, Liv B.; Sanders, Victoria C.; Tavener, Stewart J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 18 p. 3081 - 3085
反应条件
potassium fluoride; dihydrogen peroxide; potassium carbonate 1.) DMAc, 50 deg C, 30 min, 2.) DMSO, r.t.; Multistep reaction;
参考文献
Adams, Dave J.; Clark, James H.; Hansen, Liv B.; Sanders, Victoria C.; Tavener, Stewart J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 18 p. 3081 - 3085
