(三氟甲基)三甲基硅烷合成路线 （共 455 条）
反应条件
sulfur; potassium fluoride; o-di-fluorobenzene T=20°C; 0.5 h; Air;
参考文献
Chen, Chao; Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 30 p. 12454 - 12457
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100°C;
参考文献
Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2010 , vol. 132, # 21 p. 7262 - 7263
反应条件
potassium fluoride; copper(l) iodide in N,N-dimethyl-formamide T=100°C;
参考文献
Journal of the American Chemical Society, , vol. 132, # 21 p. 7262 - 7263
反应条件
1: With tetra-n-butylammonium difluorotriphenylsilicate(IV) in tetrahydrofuran T=-30 - -10°C; 2: With water in tetrahydrofuran
参考文献
MERCK SHARP and DOHME CORP.; MSD K.K.; LIN, Linus, S.; SUZUKI, Takao
Patent: WO2011/37771 A1, 2011 ;
Location in patent: Page/Page column 30-31 ;
WO 2011/037771 A1
反应条件
potassium fluoride; potassium phosphate; 1,10-phenanthroline; copper(I) bromide in N,N-dimethyl-formamide T=70°C; 4 h;
参考文献
Organic Letters, , vol. 12, # 21 p. 5060 - 5063
反应条件
potassium fluoride; potassium phosphate; 1,10-phenanthroline; copper(l) chloride in N,N-dimethyl-formamide T=70°C; 4 h;
参考文献
Organic Letters, , vol. 12, # 21 p. 5060 - 5063
反应条件
sulfur; potassium fluoride; o-di-fluorobenzene in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Chen, Chao; Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 30 p. 12454 - 12457
反应条件
sulfur; potassium fluoride; o-di-fluorobenzene in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
参考文献
Chen, Chao; Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 30 p. 12454 - 12457
反应条件
sulfur; potassium fluoride; o-di-fluorobenzene
T=20°C; 0.5 h; Air;
参考文献
Chen, Chao; Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 30 p. 12454 - 12457
反应条件
potassium fluoride; potassium phosphate; 1,10-phenanthroline; copper (I) trifluoromethane sulfonate benzene; silver carbonate in N,N-dimethyl-formamide
T=45°C; Inert atmosphere;
参考文献
Chu, Lingling; Qing, Feng-Ling
Organic Letters, 2010 , vol. 12, # 21 p. 5060 - 5063
