(三氟甲基)三甲基硅烷合成路线 （共 455 条）
反应条件
cesium fluoride in benzonitrile
T=100°C; 6 h;
参考文献
Singh, Rajendra P.; Cao, Ganfeng; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2873 - 2876
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 0.00555556 h;
参考文献
Miyake, Noriaki; Kitazume, Tomoya
Journal of Fluorine Chemistry, 2003 , vol. 122, # 2 p. 243 - 246
反应条件
cesium fluoride in neat (no solvent)
T=100°C; 6 h;
参考文献
Singh, Rajendra P.; Cao, Ganfeng; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2873 - 2876
反应条件
tris(dimethylamino)-sulphonium difluorotrimethylsilicate in Petroleum ether
T=25°C; 0.5 h; other reagent, catalysts, solvents, substrates; Product distribution;
参考文献
Kolomeitsev; Movchun; Kondratenko; Yagupolski
Synthesis, 1990 , # 12 p. 1151 - 1152
反应条件
triphenyl phosphite; cesium fluoride in benzonitrile
T=-196 - 20°C;
参考文献
Murphy-Jolly, Makeba B.; Lewis, Lesley C.; Caffyn, Andrew J. M.
Chemical Communications, 2005 , # 35 p. 4479 - 4480
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 4 h;
参考文献
Large-Radix, Sylvie; Billard, Thierry; Langlois, Bernard R.
Journal of Fluorine Chemistry, 2003 , vol. 124, # 2 p. 147 - 149
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With water in N,N-dimethyl-formamide
4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With water in N,N-dimethyl-formamide
4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With water in N,N-dimethyl-formamide
4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With water in N,N-dimethyl-formamide
4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
