反应条件
zinc in tetrahydrofuran; water under N2, at room temp., cosolvent media: H2O(NH4Cl)/THF/Zn, the alkyl tin halides were added in solvent mixt., the mixt. was maintained under N2 flow, reaction time: 22 h; Zn was filtered off, aq. phase was extd. with n-pentane, solvent was removed from organic phase, residue was distilled under vac.; (119Sn NMR monitoring);
参考文献
Journal of Organometallic Chemistry, , vol. 612, # 1-2 p. 78 - 84
