甲基N-(苄氧基)-N-甲氧基-2-甲基丙氨酸酯合成路线 （共 4 条）
反应条件
triethylamine
1.) -20 deg C, 6 h, 2.) 20 deg C, 1 h;
参考文献
Shtamburg, V. G.; Rudchenko, V. F.; Grinev, V. M.; Dmitrenko, A. A.; Pleshkova, A. P.; Kostyanovskii, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 5.1 p. 951 - 954
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 5 p. 1069 - 1072
反应条件
1: 35.3 percent / 75 h / 60 - 70 °C
2: t-BuOCl / diethyl ether / 1 h / -78 °C
3: 39.5 percent / Et3N / 1.) -78 deg C, 1h, 2.) 20 deg C, 1h
View Scheme
参考文献
Konstyanovsky, Remir G.; Rudchenko, Vladimir F.; Shtamburg, Vasilii G.; Chervin, Ivan I.; Nasibov, Shahin S.
Tetrahedron, 1981 , vol. 37, # 24 p. 4245 - 4254
反应条件
1: t-BuOCl / diethyl ether / 1 h / -78 °C
2: 39.5 percent / Et3N / 1.) -78 deg C, 1h, 2.) 20 deg C, 1h
View Scheme
参考文献
Konstyanovsky, Remir G.; Rudchenko, Vladimir F.; Shtamburg, Vasilii G.; Chervin, Ivan I.; Nasibov, Shahin S.
Tetrahedron, 1981 , vol. 37, # 24 p. 4245 - 4254
反应条件
triethylamine
1.) -78 deg C, 1h, 2.) 20 deg C, 1h;
参考文献
Konstyanovsky, Remir G.; Rudchenko, Vladimir F.; Shtamburg, Vasilii G.; Chervin, Ivan I.; Nasibov, Shahin S.
Tetrahedron, 1981 , vol. 37, # 24 p. 4245 - 4254
