您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
81331-40-0
合成路线
（共 8 条）
2270-40-8
二乙酰镳草镰刀菌烯醇
→
反应条件
81331-40-0
反应条件
1: 39 percent / SeO2 / dioxane; H2O / 24 h / Heating 2: 97 percent / pyridinium tosylate / CH2Cl2 / 24 h / Ambient temperature 3: 99 percent / 10percent aq. NaOH / methanol / 0.67 h / Ambient temperature View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
77620-47-4
→
反应条件
81331-40-0
反应条件
1: 18 percent / diisobutylaluminum hydride (DIBAH) / tetrahydrofuran; hexane / 4 h / -78 °C 2: 97 percent / pyridinium tosylate / CH2Cl2 / 24 h / Ambient temperature 3: 99 percent / 10percent aq. NaOH / methanol / 0.67 h / Ambient temperature View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
36519-25-2
新茄病镰刀菌烯醇
→
反应条件
81331-40-0
反应条件
1: 97 percent / pyridinium tosylate / CH2Cl2 / 24 h / Ambient temperature 2: 99 percent / 10percent aq. NaOH / methanol / 0.67 h / Ambient temperature View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
81331-38-6
→
反应条件
81331-40-0
反应条件
1: 33 percent / aq. NaHCO3, silver trifluoroacetate / tetrahydrofuran / 48 h / Ambient temperature 2: 97 percent / pyridinium tosylate / CH2Cl2 / 24 h / Ambient temperature 3: 99 percent / 10percent aq. NaOH / methanol / 0.67 h / Ambient temperature View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
81331-40-0
→
反应条件
81331-42-2
反应条件
1: 98 percent / triethylamine / CH2Cl2 / 17 h / 0 °C 2: 88 percent / triethylamine / CH2Cl2 / 12 h / Ambient temperature 3: 54 percent / pyridinium tosylate / aq. ethanol / 24 h / 50 °C View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
81331-40-0
→
反应条件
81331-43-3
反应条件
1: 76 percent / triethylamine / CH2Cl2 / 24 h / Ambient temperature 2: 76 percent / pyridinium tosylate / aq. ethanol / 24 h / 50 °C View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
81331-40-0
→
反应条件
77620-58-7
反应条件
1: 98 percent / triethylamine / CH2Cl2 / 17 h / 0 °C 2: 88 percent / triethylamine / CH2Cl2 / 12 h / Ambient temperature 3: 54 percent / pyridinium tosylate / aq. ethanol / 24 h / 50 °C 4: 78 percent / Me2SO, trifluoroacetic anhydride / CH2Cl2 / 0.5 h / -78 °C View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
81331-40-0
→
反应条件
77620-59-8
反应条件
1: 76 percent / triethylamine / CH2Cl2 / 24 h / Ambient temperature 2: 76 percent / pyridinium tosylate / aq. ethanol / 24 h / 50 °C 3: 77 percent / Me2SO, trifluoroacetic anhydride / CH2Cl2 / 0.5 h / -78 °C View Scheme
参考文献
Kaneko; Schmitz; Essery; Rose; Howell; O'Herron; Nachfolger; Huftalen; Bradner; Partyka; Doyle; Davies; Cundliffe
Journal of Medicinal Chemistry, 1982 , vol. 25, # 5 p. 579 - 589
