三丁基(三甲基甲硅烷基乙炔基)锡合成路线 （共 15 条）
反应条件
1: para-nitro iodo-benzene With diphenylphosphinoethane functionalized polystyrene resin-supported Pd(0) complex in N,N-dimethyl-formamide
T=20°C; Stille Cross Coupling; 0.25 h;
2: trimethyl[(tributylstannyl)ethynyl]-silane in N,N-dimethyl-formamide
T=65°C; Stille Cross Coupling; 8 h;
参考文献
Bahari, Siavash; Mohammadi-Aghdam, Babak; Molaei, Rahim; Gharibi, Zakiyeh
Canadian Journal of Chemistry, 2012 , vol. 90, # 9 p. 784 - 789
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Miller, R. D.; Reiser, O.
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 3 p. 755 - 764
反应条件
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve in dichloromethane
T=20°C; 3 h;
参考文献
Dondoni, Alessandro; Mariotti, Giandomenico; Marra, Alberto
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4475 - 4486
反应条件
in chloroform-d1
Kinetics; byproducts: (CH3)3SiCCH; react. in a NMR-tube at 23°C, addn. of the carboxylic acid soln. to the compd.; detected by NMR;
参考文献
Dallaire, Carol; Brook, Michael A.
Organometallics, 1993 , vol. 12, p. 2332 - 2338
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane
T=84°C; 2 h;
参考文献
Logue, Marshall W.; Teng, Kelly
Journal of Organic Chemistry, 1982 , vol. 47, # 13 p. 2549 - 2553
