S-2-吡啶基戊烷硫代酸酯合成路线 (共 6 条)
反应条件
nitrogen in diethyl ether -78 deg C to r.t.;
参考文献
Kim, Sunggak; Lee, Jae In; Chung, Bong Young
Journal of the Chemical Society, Chemical Communications, 1981 , # 23 p. 1231 - 1232
参考文献
Friour, G.; Alexakis, A.; Cahiez, G.; Normant, J.
Tetrahedron, 1984 , vol. 40, # 4 p. 683 - 694
反应条件
oxygen in diethyl ether 3 h; -78 deg C to r.t.;
参考文献
Kim, Sunggak; Lee, Jae In; Chung, Bong Young
Journal of the Chemical Society, Chemical Communications, 1981 , # 23 p. 1231 - 1232
反应条件
1: n-Pentanoic acid With oxalyl dichloride in dichloromethane
T=22°C; 1 h;
2: 2-mercapto-pyridine With triethylamine in dichloromethane
T=0°C; 2 h; Further stages.;
参考文献
Sung, Wook Cho; Romo, Daniel
Organic Letters, 2007 , vol. 9, # 8 p. 1537 - 1540
反应条件
in tetrahydrofuran
3 h;
参考文献
Dogutan, Dilek Kiper; Ptaszek, Marcin; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6187 - 6201
参考文献
Friour, G.; Alexakis, A.; Cahiez, G.; Normant, J.
Tetrahedron, 1984 , vol. 40, # 4 p. 683 - 694