反应条件
1: 1.) 50percent NaH-mineral oil / 1.) THF, 0 deg C, 5 min; 2.) THF
2: O3 / CD2Cl2 / -91 °C
3: CD2Cl2 / 0.28 h / -50 °C
4: 57 percent Spectr. / CD2Cl2 / 0.08 h / -50 - 25 °C
View Scheme
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
