反应条件
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 1 h, 2.) a) -78 deg C, 2 h, b) 0 deg C, 1 h
2: TsOH*H2O / benzene; H2O / 3 h / Heating
3: 1.) m-chloroperbenzoic acid, 2.) Et2NH / 1.) THF, -20 deg C, 20 min, 2.) CCl4, reflux, 10 min
View Scheme
参考文献
Gadwood, Robert C.; Lett, Renee M.
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2268 - 2275
