aluminium trichloride in neat (no solvent)
1.) 80-90 deg C, 3 h, 2.) 100 deg C, 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mahajan; Araujo
Canadian Journal of Chemistry, 1987 , vol. 65, # 1 p. 224 - 225
Cvetovich, Raymond J.; Reamer, Robert A.; DiMichele, Lisa; Chung, John Y. L.; Chilenski, Jennifer R.
Journal of Organic Chemistry, 2006 , vol. 71, # 22 p. 8610 - 8613
1: chloro(phenylmethyl)-magnesium With zinc(II) chloride in tetrahydrofuran
2: acryloyl chloride With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=0°C; 0.5 h;
Heilmann, Steven M.; Jensen, Karen M.; Krepski, Larry R.; Moren, Dean M.; Rasmussen, Jerald K.
Synthetic Communications, 1987 , vol. 17, # 7 p. 843 - 862
