2-溴-3,4-亚甲二氧基-5-甲氧基苯甲酸甲酯合成路线 (共 14 条)
反应条件
copper in N,N-dimethyl-formamide T=180°C; Ullmann coupling; 16 h;
参考文献
Alam, Ashraful; Takaguchi, Yutaka; Ito, Hideyuki; Yoshida, Takashi; Tsuboi, Sadao
Tetrahedron, 2005 , vol. 61, # 7 p. 1909 - 1918
反应条件
1: 51 percent / Cu / dimethylformamide / 3 h / Heating 2: 83 percent / 5 N NaOH / 4 h / Heating View Scheme
参考文献
Wu; Chen; Chang; Lee
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 4 p. 353 - 358
反应条件
potassium hydroxide 5 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 9 p. 2131 - 2136
反应条件
lithium aluminium tetrahydride in diethyl ether
T=0°C; 0.416667 h; Inert atmosphere;
参考文献
Altemoeller, Martina; Gehring, Timo; Cudaj, Judith; Podlech, Joachim; Goesmann, Helmut; Feldmann, Claus; Rothenberger, Alexander
European Journal of Organic Chemistry, 2009 , # 13 p. 2130 - 2140