(环戊并二烯)(五甲基环戊并二烯)二氯化锆合成路线 （共 11 条）
反应条件
in tetrahydrofuran T=-70 - 20°C;
参考文献
Wisniewska, Aleksandra; Lapczuk-Krygier, Agnieszka; Baranowska, Katarzyna; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy; Grubba, Rafal
Polyhedron, 2013 , vol. 55, p. 45 - 48
反应条件
in tetrahydrofuran T=-70 - 20°C; 25 h;
参考文献
Wisniewska, Aleksandra; Lapczuk-Krygier, Agnieszka; Baranowska, Katarzyna; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy; Grubba, Rafal
Polyhedron, 2013 , vol. 55, p. 45 - 48
反应条件
in tetrahydrofuran T=-70 - 20°C; 25 h;
参考文献
Wisniewska, Aleksandra; Lapczuk-Krygier, Agnieszka; Baranowska, Katarzyna; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy; Grubba, Rafal
Polyhedron, 2013 , vol. 55, p. 45 - 48
反应条件
in tetrahydrofuran T=-70 - 20°C;
参考文献
Wisniewska, Aleksandra; Lapczuk-Krygier, Agnieszka; Baranowska, Katarzyna; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy; Grubba, Rafal
Polyhedron, 2013 , vol. 55, p. 45 - 48
反应条件
in tetrahydrofuran
under N2, at -78 °C, stoich. amt. of educts; sublimated in vac.;
参考文献
Ewen
Journal of the American Chemical Society, 1984 , vol. 106, # 21 p. 6355 - 6364
反应条件
in toluene
addn. of anhydrous DCl gas (1 equiv) to a cold (-78°C) soln. of the Zr compound, followed by warming to room temp.; removal of volatiles under vac. and extn. of the residue with pentane allows sepn. of the products; pentane removed from the resulting filtrate to afford the aldehyde which is distd.;
参考文献
Elsner,F.H.; Woo,H.G.; Tilley,T.D.
Journal of the American Chemical Society, 1988 , vol. 110, p. 313
反应条件
hydrogenchloride in benzene-d6
condensing 1 equiv of anhyd. HCl gas to CpCp'Zr(η2-C(N-2,6-Me2C6H3)GePh3)Cl and benzene-d6 at -196°C within a NMR tube, sealing the tube, warming to 25°C yielding a pale yellow soln.; not isolated; detn. by 1H-NMR;
参考文献
Woo, Hee-Gweon; Freeman, William P.; Tilley, T. Don
Organometallics, 1992 , vol. 11, p. 2198 - 2205
参考文献
Klamo, Sara B.; Wendt, Ola F.; Henling, Larry M.; Day, Michael W.; Bercaw, John E.
Organometallics, 2007 , vol. 26, # 12 p. 3018 - 3030
参考文献
Klamo, Sara B.; Wendt, Ola F.; Henling, Larry M.; Day, Michael W.; Bercaw, John E.
Organometallics, 2007 , vol. 26, # 12 p. 3018 - 3030
参考文献
Klamo, Sara B.; Wendt, Ola F.; Henling, Larry M.; Day, Michael W.; Bercaw, John E.
Organometallics, 2007 , vol. 26, # 12 p. 3018 - 3030
