3-甲基-2,4-戊烷二酮合成路线 (共 94 条)
反应条件
copper diacetate
1) H2O, MeOH, ice-cooling, 2) CHCl3, 100 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lloris, Maria E.; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron Letters, 1990 , vol. 31, # 51 p. 7489 - 7492
反应条件
1: piperidine; ethanol
2: aqueous sulfuric acid
3: phosphoryl chloride / 210 °C
View Scheme
参考文献
Prelog et al.
Helvetica Chimica Acta, 1942 , vol. 25, p. 1654,1660
反应条件
hydrogenchloride; mercury; zinc in ethanol
参考文献
Davis,B.R. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 2820 - 2826
反应条件
copper diacetate
1) H2O, MeOH, ice-cooling, 2) CHCl3, 100 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lloris, Maria E.; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron Letters, 1990 , vol. 31, # 51 p. 7489 - 7492