4-羟基-2,2,5,5-四甲基-己烷-3-酮合成路线 （共 40 条）
反应条件
1,1-dimethylethylmagnesium chloride in diethyl ether T=-50°C; 1 h;
参考文献
Liebigs Annales, , # 1 p. 193 - 202
反应条件
chloro-trimethyl-silane; sodium in diethyl ether Heating;
参考文献
Fleming, Ian; Roberts, Richard S.; Smith, Stephen C.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 7 p. 1215 - 1228
参考文献
Synthesis, , p. 209 - 211
反应条件
silica gel in hexane; ethyl acetate
参考文献
Tetrahedron Letters, , vol. 38, # 51 p. 8903 - 8906
反应条件
1: 1.) Li, naphthalene / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 1.5 h. 2: HCl / tetrahydrofuran / 12 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 54, # 39 p. 12007 - 12028
反应条件
in diethyl ether; pentane
参考文献
Boehrer, Gerald; Knorr, Rudolf; Boehrer, Petra; Schubert, Bernhard
Liebigs Annales, 1997 , # 1 p. 193 - 202
反应条件
in diethyl ether T=-50°C; 1 h;
参考文献
Liebigs Annales, , # 1 p. 193 - 202
反应条件
mercury P=760 Torr; HeatingIrradiation; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 15 p. 3895 - 3900
反应条件
diethyl ether T=-35°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 178,180
Zhurnal Obshchei Khimii, , vol. 30, p. 1107; engl.Ausg.S.1124
反应条件
in tetrahydrofuran; diethyl ether; pentane a) -110 deg C, 2 h, 2) to r.t.;
参考文献
Journal of Organic Chemistry, , vol. 56, # 20 p. 5768 - 5773
