2,4,6-三甲氧基-3-甲基苯甲醛合成路线 （共 4 条）
反应条件
trichlorophosphate
2 h; Ambient temperature;
参考文献
Solladie, Guy; Gehrold, Nicolai; Maignan, Jean
Tetrahedron Asymmetry, 1999 , vol. 10, # 14 p. 2739 - 2747
反应条件
1: 36.9 g / phosphoryl chloride / 1.5 h / Ambient temperature
2: 21.3 g / zinc amalgam, hydrochloric acid / acetic acid; H2O / 2 h / Heating
3: 18.0 g / phosphoryl chloride / 1.5 h / Ambient temperature
View Scheme
参考文献
Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 403 - 411
反应条件
1: 21.3 g / zinc amalgam, hydrochloric acid / acetic acid; H2O / 2 h / Heating
2: 18.0 g / phosphoryl chloride / 1.5 h / Ambient temperature
View Scheme
参考文献
Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 403 - 411
反应条件
potassium carbonate; acetone
参考文献
Lloyd; Whalley
Journal of the Chemical Society, 1956 , p. 3209,3211
