1H-1,2,4-三唑-1-乙腈合成路线 (共 4 条)
反应条件
sodium hydride in tetrahydrofuran 12 h; Heating;
参考文献
Gao, Ye; Gao, Haixiang; Piekarski, Crystal; Shreeve, Jean'ne M.
European Journal of Inorganic Chemistry, 2007 , # 31 p. 4965 - 4972
反应条件
sodium ethanolate in N,N-dimethyl-formamide T=90 - 100°C; 8 h;
参考文献
Terpigorev, A. N.; Shcherbinin, M. B.; Bazanov, A. G.; Tselinskii, I. V.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 2 p. 407
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 463
反应条件
potassium hydroxide; tetrabutylammomium bromide T=20°C; 24 h;
参考文献
De la Hoz, Antonio; Blasco, Hector; Diaz-Ortiz, Angel; Elguero, Jose; Foces-Foces, Concepcion; Moreno, Andres; Sanchez-Migallon, Ana; Valiente, Gema
New Journal of Chemistry, 2002 , vol. 26, # 7 p. 926 - 932
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol
T=80°C;
参考文献
DR. REDDY'S LABORATORIES LIMITED; DR. REDDY'S LABORATORIES, INC.
Patent: WO2008/143649 A2, 2008 ;
Location in patent: Page/Page column 52 ;