1: With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; Inert atmosphere;
2: With tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
3: With hydrogenchloride; water in tetrahydrofuran; hexane
1 h;
参考文献
Chang, Yuan Jay; Chow, Tahsin J.
Tetrahedron, 2009 , vol. 65, # 24 p. 4726 - 4734