叔-丁基反式-3-戊烯酸酯合成路线 (共 4 条)
反应条件
sulfuric acid; magnesium sulfate in dichloromethane
T=20°C; 12 h; Inert atmosphere;
参考文献
Qin, Changming; Davies, Huw M. L.
Journal of the American Chemical Society, 2013 , vol. 135, # 39 p. 14516 - 14519
反应条件
potassium tert-butylate; 1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
T=28°C; other temperatures; ΔH, ΔS; Rate constantEquilibrium constantThermodynamic data;
参考文献
Hine, Jack; Kanagasabapathy, V.M.; Ng, Peter
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2745 - 2748
反应条件
potassium tert-butylate; 1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol
T=28°C; Rate constantEquilibrium constant;
参考文献
Hine, Jack; Kanagasabapathy, V.M.; Ng, Peter
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2745 - 2748
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; ammonium chloride; lithium diisopropyl amide
Yield given. Yields of byproduct given;
参考文献
Galatsis, Paul; Manwell, Jeffrey J.; Millan, Scott D.
Tetrahedron Letters, 1996 , vol. 37, # 30 p. 5261 - 5264