反应条件
1: 100 percent / n-Bu4NF / tetrahydrofuran / 2 h / 0 °C
2: Dess-Martin periodinane / CH2Cl2 / 2 h / 0 °C
3: NaClO2; NH2SO3H; Na2HPO4 / H2O; 2-methyl-propan-2-ol / 0.5 h / 20 °C
4: Et3N; DMAP; 1-hydroxybenzotriazol / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride / CH2Cl2 / 16 h / 20 °C
View Scheme
参考文献
Takao, Ken-Ichi; Yasui, Hiroyuki; Yamamoto, Shun; Sasaki, Daisuke; Kawasaki, Soujiro; Watanabe, Gohshi; Tadano, Kin-Ichi
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8789 - 8795
