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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
81721-80-4
合成路线
(共 8 条)
1018679-04-3
→
反应条件
81721-80-4
反应条件
dipyridinium dichromate in dichloromethane
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
1384384-78-4
→
反应条件
81721-80-4
反应条件
1: methanol / Photolysis; Inert atmosphere 2: dipyridinium dichromate / dichloromethane 3: hydrogenchloride / acetone 4: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
1384384-81-9
→
反应条件
81721-80-4
反应条件
1: dipyridinium dichromate / dichloromethane 2: hydrogenchloride / acetone 3: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
1384384-86-4
→
反应条件
81721-80-4
反应条件
1: hydrogenchloride / acetone 2: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
1384384-84-2
→
反应条件
81721-80-4
反应条件
1: potassium hexamethylsilazane / tetrahydrofuran / -78 °C 2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether 3: methanol / Photolysis; Inert atmosphere 4: dipyridinium dichromate / dichloromethane 5: hydrogenchloride / acetone 6: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
183198-63-2
→
反应条件
81721-80-4
反应条件
1: sodium hydride / tetrahydrofuran 2: potassium hexamethylsilazane / tetrahydrofuran / -78 °C 3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether 4: methanol / Photolysis; Inert atmosphere 5: dipyridinium dichromate / dichloromethane 6: hydrogenchloride / acetone 7: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
579-75-9
邻甲氧基苯甲酸
→
反应条件
81721-80-4
反应条件
1: thionyl chloride 2: sodium hydride / tetrahydrofuran 3: potassium hexamethylsilazane / tetrahydrofuran / -78 °C 4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether 5: methanol / Photolysis; Inert atmosphere 6: dipyridinium dichromate / dichloromethane 7: hydrogenchloride / acetone 8: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051
100-46-9
苄胺
→
反应条件
81721-80-4
反应条件
1: thionyl chloride 2: sodium hydride / tetrahydrofuran 3: potassium hexamethylsilazane / tetrahydrofuran / -78 °C 4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethylene glycol dimethyl ether 5: methanol / Photolysis; Inert atmosphere 6: dipyridinium dichromate / dichloromethane 7: hydrogenchloride / acetone 8: dipyridinium dichromate / dichloromethane View Scheme
参考文献
Dubois, Melanie; Deniau, Eric; Couture, Axel; Grandclaudon, Pierre
Synlett, 2012 , vol. 23, # 7 p. 1047 - 1051