1: in tetrahydrofuran; diethyl ether; hexane
T=0°C; 3 h;
2: With iodine in tetrahydrofuran; diethyl ether; hexane
T=20°C; 16 h; Further stages.;
参考文献
Usui, Shinya; Hashimoto, Yuichi; Morey, James V.; Wheatley, Andrew E. H.; Uchiyama, Masanobu
Journal of the American Chemical Society, 2007 , vol. 129, # 49 p. 15102 - 15103