反应条件
1: 1.) Mg, EtI / 1.) THF, a) reflux, overnight, b) RT, 1 d, 2.) THF, a) 0 deg C, 1 h, b) RT, overnight
2: 87 percent / NaN3, polyphosphoric acid / 47 °C
3: 40 percent / m-chloroperbenzoic acid / CHCl3 / 72 h / Ambient temperature
View Scheme
参考文献
Duong, Thach; Prager, Rolf H.; Were, Stephen T.
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1431 - 1440
