甲基-13C-三苯基碘化膦合成路线 （共 4 条）
参考文献
Christopher Braddock; Clarke, James; Rzepa, Henry S.
Chemical Communications, 2013 , vol. 49, # 95 p. 11176 - 11178
反应条件
triphenylphosphine in toluene
T=-10 - 20°C; 72 h; Inert atmosphere;
参考文献
Chen, Chi; Dugan, Thomas R.; Brennessel, William W.; Weix, Daniel J.; Holland, Patrick L.
Journal of the American Chemical Society, 2014 , vol. 136, # 3 p. 945 - 955
反应条件
1: PPh3[(13)C-CH3]I With dimsyl sodium in dimethyl sulfoxide
1 h;
2: acetone in dimethyl sulfoxide
T=60°C; 0.25 h;
参考文献
Harney, Matthew B.; Keaton, Richard J.; Sita, Lawrence R.
Journal of the American Chemical Society, 2004 , vol. 126, # 14 p. 4536 - 4537
反应条件
sodium hydroxide in benzene
T=40°C; 24 h; Title compound not separated from byproducts;
参考文献
Baeg, Jin-Ook; Alper, Howard
Journal of the American Chemical Society, 1994 , vol. 116, # 4 p. 1220 - 1224
