(E)-3-(2-萘基)-2-丁烯酸乙酯合成路线 （共 2 条）
反应条件
1: 95 percent / H2 / Pd/C / ethyl acetate / 760 Torr
2: 85 percent / DIBAL-H / CH2Cl2; hexane / 30 h / -78 °C
3: 80 percent / KF / propan-2-ol / 20 °C
4: 91 percent / methanesulfonyl chloride; triethylamine / CH2Cl2 / 0.33 h / 0 °C
5: 81 percent / H2O; ethyl acetate / 24 h / 50 - 55 °C
View Scheme
参考文献
Gangjee, Aleem; Yang, Jie; Queener, Sherry F.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 24 p. 8341 - 8351
反应条件
sodium hydroxide in ethanol; water
T=60°C;
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6713 - 6716
