(1S)-1,5-脱水-1-(硝基甲基)-D-山梨糖醇合成路线 (共 4 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in pyridine
T=50°C; Henry condensation; 24 h;
参考文献
Phiasivongsa, Pasit; Samoshin, Vyacheslav V.; Gross, Paul H.
Tetrahedron Letters, 2003 , vol. 44, # 29 p. 5495 - 5498
反应条件
1: With sodium methylate in methanol
2: in water
Heating;
参考文献
Baker, Kenneth W.J; March, Andrew R; Parsons, Simon; Paton, R.Michael; Stewart, Gavin W
Tetrahedron, 2002 , vol. 58, # 42 p. 8505 - 8513
参考文献
Sowden et al.
Chemistry and Industry (London, United Kingdom), 1962 , p. 1827
反应条件
sodium methylate
2.) H2O, reflux; Multistep reaction;
参考文献
Roedern, Erich Graf von; Kessler, Horst
Angewandte Chemie, 1994 , vol. 106, # 6 p. 684 - 686