1,3-二氯-1,1-二氟丙烷合成路线 （共 13 条）
反应条件
fluoro chloride; sodium hydrogensulfite T=-60°C;
参考文献
Chuvatkin, N. N.; Panteleeva, I. Yu.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 5 p. 821 - 827
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 946 - 953
反应条件
hydrogen fluoride; activated by HF amorphous Zn/chromia catalyst
T=200°C;
参考文献
INEOS FLUOR HOLDINGS LIIMITED
Patent: WO2009/125201 A2, 2009 ;
Location in patent: Page/Page column 29; 30 ;
反应条件
tri-N-butyl phosphate; iron
T=105°C; P=5149.01 Torr;
参考文献
Iikubo, Yuichi; Hedrick, Vicki; Brandstadter, Stephen M.; Cohn, Mitchel
Patent: US2004/127757 A1, 2004 ;
Location in patent: Page 7-8 ;
反应条件
bromine trifluoride; tin(IV) chloride in 1,2,2-trifluoro-trichloroethane
T=20 - 25°C;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2276 - 2278
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2522 - 2525
反应条件
chlorine
T=-70 - -50°C; im Licht;
参考文献
McBee et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 946
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 421
反应条件
hydrogenchloride; aluminium trichloride
参考文献
Myhre,P.C.; Andrews,G.D.
Journal of the American Chemical Society, 1970 , vol. 92, p. 7596 - 7597
反应条件
fluoro chloride; sodium hydrogensulfite
T=-60 - -20°C;
参考文献
Chuvatkin, N. N.; Panteleeva, I. Yu.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 5 p. 821 - 827
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 946 - 953
反应条件
antimony(V) pentachloride; SbF3
Heating;
参考文献
Nesmeyanov,A.N. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 415 - 419
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 447 - 451
反应条件
antimony dichloride trifluoride; α,α,α-trifluorotoluene; SbF3
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
反应条件
mit Licht.Irradiation;
参考文献
McBee et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 946
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 421
