1,3-二丁基-1,3-二氟二锡氧烷合成路线 （共 2 条）
反应条件
in tetrahydrofuran; dichloromethane
byproducts: (Bu4N)OSO2CH3; under N2, Schlenk setup, 1:1 mixt., Bu4NF soln. in THF added to suspn. of tin compd. in CH2Cl2 (1:1), stirred for 8-10 h at room temp.; concd., pptd. (Et2O), filtered, concd., dried (vac.), elem. anal.;
参考文献
Shankar, Ravi; Kumar, Mukesh; Chadha, Raj K.; Narula, Suraj P.
Polyhedron, 2004 , vol. 23, # 1 p. 71 - 75
反应条件
in ethanol; water
in aq. ethanol;;
参考文献
Seyferth et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2934
