alpha,alpha,alpha′,alpha′-四甲基-1,3-苯二丙酸合成路线 (共 2 条)
反应条件
potassium hydroxide in ethylene glycol T=180°C; 6 h;
参考文献
Espino, Christine G.; Fiori, Kristin Williams; Kim, Mihyong; Du Bois
Journal of the American Chemical Society, 2004 , vol. 126, # 47 p. 15378 - 15379
反应条件
1.1: LDA / tetrahydrofuran; hexane / 1.5 h / 0 °C 1.2: 75 percent / tetrahydrofuran; hexane / 10 h / 23 °C 2.1: 68 percent / KOH / ethane-1,2-diol / 6 h / 180 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 47 p. 15378 - 15379