(4-氯-2-氰基苯基)硼酸合成路线 （共 3 条）
反应条件
1: K3PO4 / Pd(PPh3)4 / dioxane; H2O / 85 °C 2: H2 View Scheme
参考文献
Boice, Genevieve N.; Savarin, Cecile G.; Murry, Jerry A.; Conrad, Karen; Matty, Louis; Corley, Edward G.; Smitrovich, Jacqueline H.; Hughes, Dave
Tetrahedron, 2004 , vol. 60, # 50 p. 11367 - 11374
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-69 - -20°C; 0.333333 h;
参考文献
Boice, Genevieve N.; Savarin, Cecile G.; Murry, Jerry A.; Conrad, Karen; Matty, Louis; Corley, Edward G.; Smitrovich, Jacqueline H.; Hughes, Dave
Tetrahedron, 2004 , vol. 60, # 50 p. 11367 - 11374
反应条件
1: 63 percent / TFA; H2SO4; 1,3-dibromo-5,5-dimethylhydantoin / 6 h / 24 - 31 °C
2: 69 percent / triisopropyl borate; n-BuLi / tetrahydrofuran; hexane / 0.33 h / -69 - -20 °C
View Scheme
参考文献
Boice, Genevieve N.; Savarin, Cecile G.; Murry, Jerry A.; Conrad, Karen; Matty, Louis; Corley, Edward G.; Smitrovich, Jacqueline H.; Hughes, Dave
Tetrahedron, 2004 , vol. 60, # 50 p. 11367 - 11374
