1,2-二氨基-4,5-亚乙基二氧基苯合成路线 （共 8 条）
参考文献
Xuanzhu Pharma Co., Ltd.
Patent: EP2532665 A1, 2012 ;
Location in patent: Page/Page column 30 ;
反应条件
hydrogen; palladium 10 on activated carbon in methanol
18 h;
参考文献
Xuanzhu Pharma Co., Ltd.
Patent: EP2532665 A1, 2012 ;
Location in patent: Page/Page column 30 ;
反应条件
potassium hydroxide in ethanol
4 h; Heating;
参考文献
Mateu; Capilla; Harrak; Pujol
Tetrahedron, 2002 , vol. 58, # 26 p. 5241 - 5250
反应条件
hydrogen in ethanol
P=22801.5 Torr;
参考文献
Kim, Dong Wan; Kim, Junghwan; Hwang, Jaeyoung; Choi, Myong Yong; Kim, Jae Sang
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 8 p. 2643 - 2647
反应条件
1: nitric acid; acetic acid / 3 h / 0 - 20 °C
2: sulfuric acid / 6 h / Reflux
3: hydrogen / palladium 10 on activated carbon / methanol / 18 h
View Scheme
参考文献
Xuanzhu Pharma Co., Ltd.
Patent: EP2532665 A1, 2012 ;
反应条件
1: 3 h / 20 °C
2: nitric acid; acetic acid / 3 h / 0 - 20 °C
3: sulfuric acid / 6 h / Reflux
4: hydrogen / palladium 10 on activated carbon / methanol / 18 h
View Scheme
参考文献
Xuanzhu Pharma Co., Ltd.
Patent: EP2532665 A1, 2012 ;
反应条件
1: sulfuric acid / 6 h / Reflux
2: hydrogen / palladium 10 on activated carbon / methanol / 18 h
View Scheme
参考文献
Xuanzhu Pharma Co., Ltd.
Patent: EP2532665 A1, 2012 ;
反应条件
1: nitric acid; acetic anhydride
2: hydrogen / ethanol / 22801.5 Torr
View Scheme
参考文献
Kim, Dong Wan; Kim, Junghwan; Hwang, Jaeyoung; Choi, Myong Yong; Kim, Jae Sang
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 8 p. 2643 - 2647
