2,2,2-三氯乙酰胺苄酯合成路线 （共 52 条）
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane T=-15 - 25°C; 1 h;
参考文献
Patil, Vijay J.
Tetrahedron Letters, 1996 , vol. 37, # 9 p. 1481 - 1484
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane 2.5 h; Ambient temperature;
参考文献
Widmer, Ulrich
Synthesis, 1987 , # 6 p. 568 - 570
反应条件
Yield given. Multistep reaction;
参考文献
Wang, Jidong; Okada, Yoshio; Li, Wei; Yokoi, Toshio; Zhu, Jintao
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 621 - 624
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane T=20°C;
参考文献
Xie, Yuanzhen; Wang, Ning; Cheng, Bin; Zhai, Hongbin
Organic Letters, 2012 , vol. 14, # 1 p. 3 - 5
反应条件
1: 79 percent / CF3SO3H / CH2Cl2; cyclohexane / Ambient temperature 2: 1) aq. KOH, 2) I2, KI, 3) 1,4-diazabicyclo<2.2.2>octane / 1) MeOH, r.t., 2) H2O, hexane, EtOAc, r.t., 1 h, 3) DMSO, 132-140 deg C, 15 min 3: diisobutylaluminium hydride / CH2Cl2 / 0 °C View Scheme
参考文献
Daniewski; Wovkulich; Uskokovic
Journal of Organic Chemistry, 1992 , vol. 57, # 26 p. 7133 - 7139
反应条件
1: acid 2: lithium aluminium hydride 3: CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Chakraborty, Tushar Kanti; Mohan, Bajjuri Krishna; Sreekanth, Midde
Tetrahedron Letters, 2006 , vol. 47, # 29 p. 5003 - 5005
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane T=20°C; 12 h;
参考文献
Hernandez-Torres, Gloria; Carreno, M. Carmen; Urbano, Antonio; Colobert, Franacoise
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1283 - 1293
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane 0.5 h; Ambient temperature;
参考文献
Synthesis, , # 6 p. 568 - 570
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane 24 h; Ambient temperature;
参考文献
Kokotos, George; Chiou, Antonia
Synthesis, 1997 , # 2 p. 168 - 170
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane
参考文献
Baer, Hans H.; Shen, Yaping; Wu, Xinfu
Carbohydrate Research, 1993 , vol. 241, p. 117 - 130
