2,2,2-三氯乙酰胺苄酯合成路线 （共 52 条）
反应条件
trifluorormethanesulfonic acid in tetrachloromethane; cyclohexane T=20°C; 2.5 h; Title compound not separated from byproducts;
参考文献
Van Zijl, Anthoni W.; Lopez, Fernando; Minnaard, Adriaan J.; Feringa, Ben L.
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2558 - 2563
反应条件
1: With trifluorormethanesulfonic acid in tetrachloromethane; cyclohexane T=20°C; 2.5 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Van Zijl, Anthoni W.; Lopez, Fernando; Minnaard, Adriaan J.; Feringa, Ben L.
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2558 - 2563
反应条件
1.1: 52 percent / TMSOTf / cyclohexane / 20 °C 2.1: cesium fluoride / dimethylformamide / 16 h / 20 °C 2.2: 82 percent / NH4Cl; aq. HCl / diethyl ether; dimethylformamide View Scheme
参考文献
Maleczka Jr., Robert E.; Geng, Feng
Organic Letters, 1999 , vol. 1, # 7 p. 1111 - 1113
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane T=25°C; 2 h;
参考文献
Boger; Hong
Journal of the American Chemical Society, 2001 , vol. 123, # 35 p. 8515 - 8519
反应条件
1: 11.8 mmol / CF3SO3H / tetrahydrofuran / 18 h / 20 °C 2: 98 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 23 °C View Scheme
参考文献
Weghe, P. Van de; Bied, C.; Collin, J.; Marcalo, J.; Santos, I.
Journal of Organometallic Chemistry, 1994 , vol. 475, # 1-2 p. 121 - 126
反应条件
trifluorormethanesulfonic acid in dichloromethane T=0 - 20°C;
参考文献
WO2008/119804 A1, ;
Page/Page column 63-64 ;
WO 2008/119804 A1
反应条件
trifluorormethanesulfonic acid in dichloromethane; cyclohexane 18 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 7 p. 2094 - 2101
反应条件
trifluorormethanesulfonic acid in cyclohexane 1 h;
参考文献
Barrett, Anthony G. M.; Pilipauskas, Daniel
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5170 - 5173
反应条件
trifluorormethanesulfonic acid in dichloromethane T=20°C; Cooling with iceInert atmosphere;
参考文献
Kowa Company. Ltd.
Patent: EP2098515 A1, 2009 ;
Location in patent: Page/Page column 77 ;
反应条件
silver trifluoromethanesulfonate; gold(I) chloride in benzene 0.5 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2533 - 2535
