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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
81965-50-6
合成路线
（共 7 条）
81965-50-6
→
反应条件
2541-61-9
9,12-十八碳二烯醛
反应条件
1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C / under N2 2: 30percent H3PO4 / methanol / 5 h / Ambient temperature 3: CrO3, conc H2SO4 / H2O; acetone / 0.5 h / 0 °C 4: LCA(long chain aldehydes)-forming activity in Ulva pertusa fronds solubilized by Triton X-100, 2,4-dinitrophenylhydrazone / 0.25 h / 35 °C View Scheme
参考文献
Kajiwara, Tadahiko; Yoshikawa, Hiroshi; Matsui, Kenji; Hatanaka, Akikazu; Kawai, Tetsuo
Phytochemistry (Elsevier), 1989 , vol. 28, # 2 p. 407 - 410
81965-50-6
→
反应条件
29204-20-4
DELTA10顺式-13九癸二烯酸
反应条件
1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C / under N2 2: 30percent H3PO4 / methanol / 5 h / Ambient temperature 3: CrO3, conc H2SO4 / H2O; acetone / 0.5 h / 0 °C View Scheme
参考文献
Kajiwara, Tadahiko; Yoshikawa, Hiroshi; Matsui, Kenji; Hatanaka, Akikazu; Kawai, Tetsuo
Phytochemistry (Elsevier), 1989 , vol. 28, # 2 p. 407 - 410
81965-50-6
→
反应条件
43047-93-4
反应条件
polymethylhydroxysiloxane; zinc(II) chloride in diethyl ether 20 h; Ambient temperature;
参考文献
Chandrasekhar; Ravindra Reddy; Ramarao
Synthetic Communications, 1997 , vol. 27, # 13 p. 2251 - 2254
81965-50-6
→
反应条件
56797-42-3
反应条件
1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C / under N2 2: 30percent H3PO4 / methanol / 5 h / Ambient temperature 3: CrO3, conc H2SO4 / H2O; acetone / 0.5 h / 0 °C 4: LCA(long chain aldehydes)-forming activity in Ulva pertusa fronds solubilized by Triton X-100, 2,4-dinitrophenylhydrazone / 0.25 h / 35 °C 5: LCA(long chain aldehydes)-forming activity in Ulva pertusa fronds solubilized by Triton X-100 / 0.25 h / 35 °C View Scheme
参考文献
Kajiwara, Tadahiko; Yoshikawa, Hiroshi; Matsui, Kenji; Hatanaka, Akikazu; Kawai, Tetsuo
Phytochemistry (Elsevier), 1989 , vol. 28, # 2 p. 407 - 410
81965-50-6
→
反应条件
62232-88-6
反应条件
1: diethyl ether 2: Et3SiH, CF3CO2H 3: NaOH / methanol 4: (COCl)2, DMSO, Et3N / CH2Cl2 View Scheme
参考文献
Furukawa, Yoshiaki; Yamagiwa, Yoshiro; Kamikawa, Tadao
Journal of the Chemical Society, Chemical Communications, 1986 , # 16 p. 1234 - 1235
81965-50-6
→
反应条件
62607-69-6
10-苯基-1-癸醇
反应条件
1: diethyl ether 2: Et3SiH, CF3CO2H 3: NaOH / methanol View Scheme
参考文献
Furukawa, Yoshiaki; Yamagiwa, Yoshiro; Kamikawa, Tadao
Journal of the Chemical Society, Chemical Communications, 1986 , # 16 p. 1234 - 1235
558-13-4
四溴化碳
+
81965-50-6
→
反应条件
544476-90-6
反应条件
triethylamine; triphenylphosphine in dichloromethane
参考文献
Hakogi, Toshikazu; Shigenari, Toshihiko; Katsumura, Shigeo; Sano, Takamitsu; Kohno, Takayuki; Igarashi, Yasuyuki
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 4 p. 661 - 664
