1,3-二氧杂环戊烯并[4,5-g]异喹啉-5-醇,5,6,7,8-四氢-4-甲氧基-6-甲基-合成路线 （共 19 条）
反应条件
hydrogenchloride; zinc
参考文献
Pyman; Remfry
Journal of the Chemical Society, 1912 , vol. 101, p. 1607
反应条件
isobutyramide; triethylamine
T=160°C; 0.333333 h;
参考文献
Krasnov; Kartsev; Khrustalev
Russian Chemical Bulletin, 2002 , vol. 51, # 8 p. 1540 - 1544
反应条件
Multi-step reaction with 6 steps 1: 99 percent / H2 / 5percent Pd-C / ethanol2: 78 percent / 6N HCl3: 99 percent / CH2Cl2 / 1 h / Ambient temperature4: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C5: I2, potassium acetate / ethanol / 3 h / Heating6: 25percent NaOH, sodium sulfite / H2O / 1) 1h, 40 deg C, 2) 1h, 20 deg C
参考文献
Shirasaka, Tadashi; Takuma, Yuki; Shimpuku, Tetsuro; Imaki, Naoshi Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3767 - 3771
反应条件
Multi-step reaction with 3 steps 1: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C2: I2, potassium acetate / ethanol / 3 h / Heating3: 25percent NaOH, sodium sulfite / H2O / 1) 1h, 40 deg C, 2) 1h, 20 deg C
参考文献
Shirasaka, Tadashi; Takuma, Yuki; Shimpuku, Tetsuro; Imaki, Naoshi Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3767 - 3771
反应条件
Multi-step reaction with 4 steps 1: 99 percent / CH2Cl2 / 1 h / Ambient temperature2: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C3: I2, potassium acetate / ethanol / 3 h / Heating4: 25percent NaOH, sodium sulfite / H2O / 1) 1h, 40 deg C, 2) 1h, 20 deg C
参考文献
Shirasaka, Tadashi; Takuma, Yuki; Shimpuku, Tetsuro; Imaki, Naoshi Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3767 - 3771
反应条件
Multi-step reaction with 5 steps 1: 78 percent / 6N HCl2: 99 percent / CH2Cl2 / 1 h / Ambient temperature3: 95 percent / H2 / 5percent Pd-C / ethanol / 7 h / 50 °C4: I2, potassium acetate / ethanol / 3 h / Heating5: 25percent NaOH, sodium sulfite / H2O / 1) 1h, 40 deg C, 2) 1h, 20 deg C
参考文献
Shirasaka, Tadashi; Takuma, Yuki; Shimpuku, Tetsuro; Imaki, Naoshi Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3767 - 3771
反应条件
With manganese(IV) oxide; sulfuric acid
参考文献
Woehler Justus Liebigs Annalen der Chemie, 1844 , vol. 50, p. 1,19 Beckett; Wright Journal of the Chemical Society, 1875 , vol. 28, p. 580,581
反应条件
With ethanol Erhitzen des Reaktionsprodukts auf Siedetemperatur;
参考文献
Hope; Robinson Journal of the Chemical Society, 1911 , vol. 99, p. 1168
反应条件
With sodium hydrogensulfite
参考文献
Beke; Martos-Barczai Acta Chimica Academiae Scientiarum Hungaricae, 1957 , vol. 11, p. 295,298Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1836,1838; engl. Ausg. S. 1901, 1903
