2-甲基-1,5-己二烯-3-炔合成路线 （共 26 条）
反应条件
1: HgSO4; H2SO4; methanol / anschl. mit wss. H3PO4 2: Raney nickel; ethanol / 85 °C / 73550.8 Torr / Hydrogenation 3: oxalic acid / 140 °C View Scheme
参考文献
Koperina et al.
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1498,1500
Chem.Abstr., 1951 , p. 2417
反应条件
1: HgSO4; H2SO4; methanol / anschl. mit wss. H3PO4 2: Raney nickel; ethanol / 85 °C / 73550.8 Torr / Hydrogenation 3: oxalic acid / 140 °C 4: palladium/charcoal / Hydrogenation View Scheme
参考文献
Koperina et al.
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1498,1500
Chem.Abstr., 1951 , p. 2417
反应条件
1: HgSO4; H2SO4; methanol / anschl. mit wss. H3PO4 2: platinum/charcoal / Hydrogenation View Scheme
参考文献
Koperina et al.
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1498,1500
Chem.Abstr., 1951 , p. 2417
反应条件
ion-exchange resin KU-23
T=30°C; Dehydration; P=100 Torr; 2 h;
参考文献
Grigorev; Kozhevnikov
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 4 p. 214 - 215
反应条件
phosphoric acid
T=65 - 80°C; P=15 - 20 Torr;
参考文献
Nasarow; Romanow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1940 , p. 568
Chem.Abstr., 1941 , p. 4735
反应条件
potassium hydroxide; N-phenyl-N-β-naphthylamine in methanol
参考文献
Mkryan,G.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1682 - 1685
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 1810 - 1814
反应条件
potassium hydroxide; N-phenyl-N-β-naphthylamine in methanol
参考文献
Mkryan,G.M. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1682 - 1685
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 1810 - 1814
参考文献
Kheruze,Yu.I.; Petrov,A.A.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2528 - 2533,2511 - 2515
反应条件
water; ammonium chloride; copper(l) chloride
参考文献
Nasarow; Janbikow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1942 , p. 66
Chem.Abstr., 1943 , p. 2345
反应条件
potassium hydroxide; acetone
参考文献
Nasarow; Kusnezowa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1941 , p. 431,438
Chem.Abstr., 1942 , p. 1296
